Triethylamine → 4-Fluorophenyl 2-propenoate
反応式
[C:1](Cl)(=[O:4])[CH:2]=[CH2:3].[F:6][C:7]1[CH:12]=[CH:11][C:10]([OH:13])=[CH:9][CH:8]=1.C(N(CC)CC)C>ClCCl>[C:1]([O:13][C:10]1[CH:11]=[CH:12][C:7]([F:6])=[CH:8][CH:9]=1)(=[O:4])[CH:2]=[CH2:3]参加物
5
実験手順
For example: Acryloyl chloride and 4-fluorophenol react in dichloromethane in the presence of triethylamine to give 4-fluorophenyl acrylate 10 (R=4-fluorophenyl). Compound 10 is then added to a solution of 9 in ethanol and diethylamine to give 11 (R=4-fluorophenyl) after usual workup.
出典と根拠
- ORDレコード
- ord-d38970563fa0408ebb79c6acb5e4884d
- 出典データセット
- uspto-grants-2011_05
- 特許番号
- USRE042412E1
反応ノート
読み込み中…