Methyl iodide → 2-Iodo-3-methoxy-6-methylpyridine
反応式
[OH:1][C:2]1[C:3]([I:9])=[N:4][C:5]([CH3:8])=[CH:6][CH:7]=1.I[CH3:11]>>[I:9][C:3]1[C:2]([O:1][CH3:11])=[CH:7][CH:6]=[C:5]([CH3:8])[N:4]=1参加物
3
実験手順
Under the conditions of example 1 D, 10 g of 3-hydroxy-2-iodo-6-methylpyridine is reacted with 2.7 ml of iodomethane and worked up. 10.5 g of 2-iodo-3-methoxy-6-methylpyridine of melting point 45°-50° C. is obtained.
出典と根拠
- ORDレコード
- ord-f38c2634453445cb9ddfca9735a75e3d
- 出典データセット
- uspto-grants-1997_04
- 特許番号
- US05624943
反応ノート
読み込み中…