Methyl iodide → 5-Fluoro-2,3-dimethyl-benzothiazol-3-ium iodide

HRID 557137

反応式

HRID 557137 の反応式
[F:1][C:2]1[CH:3]=[CH:4][C:5]2[S:9][C:8]([CH3:10])=[N:7][C:6]=2[CH:11]=1.[I:12][CH3:13]>C(O)C>[I-:12].[F:1][C:2]1[CH:3]=[CH:4][C:5]2[S:9][C:8]([CH3:10])=[N+:7]([CH3:13])[C:6]=2[CH:11]=1

参加物

4

反応物 2

HCID 6328Methyl iodideHCID 5974375-Fluoro-2-methylbenzothiazole

生成物 1

HCID 669907845-Fluoro-2,3-dimethyl-benzothiazol-3-ium iodide

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

13.0 g (10.4 ml, 77.7 mmol) 5-Fluoro-2-methyl-benzothiazole and 22.1 g (9.47 ml, 156 mmol) iodomethane were boiled in ethanol for 7 h. The residue was filtrated. 4.00 g=17% white powder

後処理

  1. filtrationThe residue was filtrated

出典と根拠

ORDレコード
ord-ca4303ac31c042c0bca4858ea5b4ad7a
出典データセット
uspto-grants-2011_11
特許番号
US08058431B2

関連ノート

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