Iodine → 1,2-Dihydro-2,2,4-trimethylquinoline-6-carboxylic acid methyl ester
反応式
[NH2:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:4][CH:3]=1.II>O=C(C=C(C)C)C>[CH3:9][O:8][C:6]([C:5]1[CH:10]=[C:11]2[C:2](=[CH:3][CH:4]=1)[NH:1][C:5]([CH3:10])([CH3:6])[CH:4]=[C:3]2[CH3:2])=[O:7]参加物
4
実験手順
Skraup reaction of methyl 4-aminobenzoate (5.0 g) and iodine (1.7 g) in mesityl oxide (25 ml) was performed according to the method described in example 1.
出典と根拠
- ORDレコード
- ord-1c4c78c8384c42e0ba114e4b06857ed8
- 出典データセット
- uspto-grants-2011_11
- 特許番号
- US08058441B2
反応ノート
読み込み中…