2-(Trifluoromethyl)benzoic acid → 2-(Methylthio)-6-(trifluoromethyl)benzoic acid
反応式
[F:1][C:2]([F:13])([F:12])[C:3]1[CH:11]=[CH:10][CH:9]=[CH:8][C:4]=1[C:5]([OH:7])=[O:6].[CH3:14][S:15]SC>>[CH3:14][S:15][C:8]1[CH:9]=[CH:10][CH:11]=[C:3]([C:2]([F:12])([F:13])[F:1])[C:4]=1[C:5]([OH:7])=[O:6]参加物
3
実験手順
The title compound, white solid, MS: m/e=191.1 [(M−CO2H)−], was prepared in accordance with the general method of intermediate E from 2-(trifluoromethyl)benzoic acid and dimethyl disulfide.
出典と根拠
- ORDレコード
- ord-4db86d3c0b4a41b598e867f8c7702f75
- 出典データセット
- uspto-grants-2011_11
- 特許番号
- US08063098B2
反応ノート
読み込み中…