4-(Trifluoromethyl)benzoic acid → Benzoic acid, 2-(methylthio)-4-(trifluoromethyl)-

反応式

[F:1][C:2]([F:13])([F:12])[C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1.[CH3:14][S:15]SC>>[CH3:14][S:15][C:10]1[CH:11]=[C:3]([C:2]([F:12])([F:13])[F:1])[CH:4]=[CH:5][C:6]=1[C:7]([OH:9])=[O:8]

参加物

反応物 2

HCID 99664-(Trifluoromethyl)benzoic acid

HCID 12232Dimethyl Disulfide

生成物 1

HCID 11085762Benzoic acid, 2-(methylthio)-4-(trifluoromethyl)-

実験手順

The title compound, white solid, MS: m/e=235.0 [(M−H)−], was prepared in accordance with the general method of intermediate E from 4-(trifluoromethyl)benzoic acid and dimethyl disulfide.

出典と根拠

ORDレコード: ord-d4a345fc147b46d393bbc2af7b9c10b6
出典データセット: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08063098B2

反応ノート

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