化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → 2,2,4,4,6,6-Hexamethylcyclotrisilazane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | Dichlorodimethylsilane | HCID 6398 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 2,2,4,4,6,6-Hexamethylcyclotrisilazane | HCID 66094 | — |
反応手順
This method involves reacting dimethyldichlorosilane with ammonia in benzene at 30° C., removing ammonia chloride by-product by filtration through a glass filter or the like, and distilling the reaction product to isolate hexamethylcyclotrisilazane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05245066 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-c1c083a6f395481abe3df8731345c900 |
| 出典メモ | uspto-grants-1993_09 |