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HRID5617

反应详情

EQUATION

反应方程式

HRID 5617 的结构方程式

REACTANTS

反应物

2
结构：N
HCID222

Ammonia gas

H3N

结构：C[Si](C)(Cl)Cl
HCID6398

Dimethyldichlorosilane

C2H6Cl2Si

PRODUCTS

生成物

1
结构：C[Si]1(C)N[Si](C)(C)N[Si](C)(C)N1
HCID66094

2,2,4,4,6,6-Hexamethylcyclotrisilazane

C6H21N3Si3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

This method involves reacting dimethyldichlorosilane with ammonia in benzene at 30° C., removing ammonia chloride by-product by filtration through a glass filter or the like, and distilling the reaction product to isolate hexamethylcyclotrisilazane.

WORKUP

后处理

  1. customat 30° C.
  2. customremoving ammonia chloride by-product
  3. filtrationby filtration through a glass
  4. filtrationfilter
  5. distillationthe like, and distilling the reaction product