反応式
[CH:1]1([O:7][CH2:8][C:9]([OH:11])=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl:12]SCl>>[CH:1]1([O:7][CH2:8][C:9]([Cl:12])=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1参加物
3
実験手順
A mixture of 2-(cyclohexyloxy)acetic acid (0.90 g, 5.69 mmol) and dichlorosulfane (10 mL) was refluxed for 2 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound as yellow oil, which was used for next step without further purification.
後処理
- temperaturewas refluxed for 2 h
- concentrationconcentrated in vacuo
出典と根拠
- ORDレコード
- ord-8af8cc706d3a457badbaab90d0f5f777
- 出典データセット
- uspto-grants-2016_09
- 特許番号
- US09434695B2
関連ノート
読み込み中…