Ammonia → N-(3-Chlorophenyl)benzenemethanamine
反応式
C(C(C(C(O)=O)O)O)(O)=O.[Cl:11][C:12]1[CH:13]=[C:14]([NH:18][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:15]=[CH:16][CH:17]=1.N>C(Cl)(Cl)Cl>[Cl:11][C:12]1[CH:13]=[C:14]([NH:18][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:15]=[CH:16][CH:17]=1参加物
4
実験手順
Next, (+)-(3-chlorophenyl)phenylmethylamine (+)tartrate (4.28 g) was suspended in chloroform (40 ml), and 28%-aqueous ammonia was added thereto to neutralize the mixture. Thereafter, the chloroform layer was separated therefrom. The extract was dried over anhydrous magnesium sulfate, and the solvent was removed by evaporation in vacuo, to give (+)-(3-chlorophenyl)phenylmethylamine (2.45 g) as a pale yellow oil.
後処理
- customThereafter, the chloroform layer was separated
- dry with materialThe extract was dried over anhydrous magnesium sulfate
- customthe solvent was removed by evaporation in vacuo
出典と根拠
- ORDレコード
- ord-c26e0cf2cd824304818775200eedf1f3
- 出典データセット
- uspto-grants-2001_01
- 特許番号
- US06172228B2
反応ノート
読み込み中…