Nitric Acid → 1,3-Dicyclopropylmethyl-8-nitro xanthine

HRID 568147

反応式

HRID 568147 の反応式
C1(CN2C(=O)C3NC(N)=NC=3N(CC3CC3)C2=O)CC1.[CH:21]1([CH2:24][N:25]2[C:34](=[O:35])[C:33]3[NH:32][CH:31]=[N:30][C:29]=3[N:28]([CH2:36][CH:37]3[CH2:39][CH2:38]3)[C:26]2=[O:27])[CH2:23][CH2:22]1.[N+:40]([O-])([OH:42])=[O:41]>>[CH:21]1([CH2:24][N:25]2[C:34](=[O:35])[C:33]3[NH:32][C:31]([N+:40]([O-:42])=[O:41])=[N:30][C:29]=3[N:28]([CH2:36][CH:37]3[CH2:39][CH2:38]3)[C:26]2=[O:27])[CH2:23][CH2:22]1

参加物

4

反応物 3

HCID 944Nitric AcidHCID 71356CipamfyllineHCID 152913031,3-Dicyclopropylmethyl xanthine

生成物 1

HCID 98576581,3-Dicyclopropylmethyl-8-nitro xanthine

実験手順

A process for making 1,3-dicyclopropylmethyl-8-amino xanthine which process comprises reacting 1,3-dicyclopropylmethyl xanthine with nitric acid to yield 1,3-dicyclopropylmethyl-8-nitro xanthine and thereafter reducing the nitro group to an amino group to yield 1,3-dicyclopropylmethyl-8-amino xanthine.

出典と根拠

ORDレコード
ord-5b88cf8b868a4a33b736bc9810a8ac53
出典データセット
uspto-grants-2001_01
特許番号
US06180791B2

関連ノート

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