Sulfamide → HCID 178479209、化合物

HRID 569276

反応式

HRID 569276 の反応式
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].Cl.[Cl:7][CH2:8][CH2:9][C:10]#[N:11]>C(OCC)C>[ClH:7].[S:1]([NH:5][C:10](=[NH:11])[CH2:9][CH2:8][Cl:7])(=[O:3])(=[O:2])[NH2:4]

参加物

4

反応物 2

HCID 82267SulfamideHCID 867420433-Chloropropionitrile hydrogen chloride

生成物 1

HCID 178479209HCID 178479209、化合物

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.

後処理

  1. additionTo a stirred suspension of 9.61 g
  2. filtrationthe product is filtered off
  3. washwashed twice with acetone
  4. customdried

出典と根拠

ORDレコード
ord-3edc6a87650c40d881e2ef0137c4c5f3
出典データセット
uspto-grants-1988_03
特許番号
US04731479

関連ノート

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