Sulfamide → HCID 178479209、化合物
反応式
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].Cl.[Cl:7][CH2:8][CH2:9][C:10]#[N:11]>C(OCC)C>[ClH:7].[S:1]([NH:5][C:10](=[NH:11])[CH2:9][CH2:8][Cl:7])(=[O:3])(=[O:2])[NH2:4]参加物
4
実験手順
To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.
後処理
- additionTo a stirred suspension of 9.61 g
- filtrationthe product is filtered off
- washwashed twice with acetone
- customdried
出典と根拠
- ORDレコード
- ord-3edc6a87650c40d881e2ef0137c4c5f3
- 出典データセット
- uspto-grants-1988_03
- 特許番号
- US04731479
反応ノート
読み込み中…