Glycine → HCID 10176752、化合物
反応式
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].[C:6](Cl)(=[O:15])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[OH-].[Na+]>O.CCOCC>[C:6]([NH:1][CH2:2][C:3]([OH:5])=[O:4])(=[O:15])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]参加物
6
実験手順
Glycine (20 mmol) was reacted with nonanoyl chloride (22 ml) in the presence of NaOH (40 mmol) in a mixture of water and ether as described in Example 1 Part A. The crude crystalline product (4.25 g) was recrystallized from ethyl acetate (40-50 ml) to give the title compound (3.42 g, 79.5%), m.p. 106°-109° C.
後処理
- customThe crude crystalline product (4.25 g) was recrystallized from ethyl acetate (40-50 ml)
出典と根拠
- ORDレコード
- ord-53df7cdd58d64abcbaffbf5a5604cb7b
- 出典データセット
- uspto-grants-1988_03
- 特許番号
- US04734424
反応ノート
読み込み中…