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Water → Adipic acid di(2-propylidene hydrazide)

HRID 578613
ノート
印刷プレビュー

反応式

HRID 578613 の反応式
O.[C:2]([NH:12][NH2:13])(=[O:11])[CH2:3][CH2:4][CH2:5][CH2:6][C:7]([NH:9][NH2:10])=[O:8]>CC(=O)C>[CH:2](=[N:10][NH:9][C:7](=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][C:2]([NH:12][N:13]=[CH:5][CH2:6][CH3:7])=[O:11])[CH2:3][CH3:4]
参加物実験手順後処理出典と根拠反応ノート

参加物

4

反応物 2

HCID 962WaterHCID 66117Adipic Dihydrazide

生成物 1

HCID 86666342Adipic acid di(2-propylidene hydrazide)

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

In a stainless steel flask equipped with an agitator, 58.6 grams of water were added, the agitator was turned on, then 25 grams of adipic acid dihydrazide were added. The mixture was agitated for at least 10 minutes until a stable dispersion was formed. 16.4 grams of 2-propanone were then added under mixing. A clear solution formed after a few minutes. Mixing was continued for at least another hour until reaction product precipitated and formed a stable dispersion.

後処理

  1. additionwere added
  2. additionwere added
  3. customwas formed
  4. additionunder mixing
  5. customA clear solution formed after a few minutes
  6. additionMixing
  7. customuntil reaction product
  8. customprecipitated
  9. customformed a stable dispersion

出典と根拠

ORDレコード
ord-59e99d01d81845d1a2b7979ebe0a412e
出典データセット
uspto-grants-2015_05
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US09040617B2

反応ノート

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