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Sodium hydride → HCID 70414521、化合物

HRID 579758
ノート
印刷プレビュー

反応式

HRID 579758 の反応式
[H-].[Na+].[CH3:3][C:4]1[N:5]([CH2:9][CH:10]2[C:22](=[O:23])[C:21]3[C:20]4[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=4)[NH:14][C:13]=3[CH2:12][CH2:11]2)[CH:6]=[CH:7][N:8]=1.[CH3:24][S:25](Cl)(=[O:27])=[O:26].[C:29]([OH:36])(=[O:35])/[CH:30]=[CH:31]\[C:32]([OH:34])=[O:33]>CN(C)C=O.C(O)C.CCOCC>[C:29]([OH:36])(=[O:35])/[CH:30]=[CH:31]\[C:32]([OH:34])=[O:33].[CH3:3][C:4]1[N:5]([CH2:9][CH:10]2[C:22](=[O:23])[C:21]3[C:20]4[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=4)[N:14]([S:25]([CH3:24])(=[O:27])=[O:26])[C:13]=3[CH2:12][CH2:11]2)[CH:6]=[CH:7][N:8]=1
参加物実験手順後処理出典と根拠反応ノート

参加物

8

反応物 4

HCID 24758Sodium hydrideHCID 31297Methanesulfonyl chlorideHCID 444266Maleic AcidHCID 108912241,2,3,9-Tetrahydro-3-[(2-methyl-1H-imidazol-1-yl)methyl]-4H-carbazol-4-one

生成物 1

HCID 70414521HCID 70414521、化合物

試薬・触媒・溶媒 3

HCID 702Ethanol溶媒2 回
HCID 3283Diethyl Ether溶媒
HCID 6228Dimethylformamide溶媒

実験手順

Sodium hydride (0.075 g) was added to a solution of 1,2,3,9-tetrahydro-3-[(2-methyl-1H-imidazol-1-yl)methyl]-4H-carbazol-4-one (0.7 g) in dimethylformamide (10 ml) and the mixture was stirred for 30 min. Methanesulphonyl chloride (0.25 ml) was added and stirring continued at room temperature for 5 h. The resulting solution was partitioned between sodium carbonate (100 ml) and ethyl acetate (3×50 ml). The combined organic layers were washed with water (3×50 ml), dried (Na2SO4), and evaporated in vacuo to give an oil. Purification by flash chromatography (A) gave an oil, which was dissolved in ethanol (10 ml) and added to a solution of maleic acid (0.15 g) in ethanol (5 ml). Addition of dry ether precipitated the title compound (0.7 g) m.p. 141°-142.5°.

後処理

  1. stirringstirring
  2. waitcontinued at room temperature for 5 h
  3. customThe resulting solution was partitioned between sodium carbonate (100 ml) and ethyl acetate (3×50 ml)
  4. washThe combined organic layers were washed with water (3×50 ml)
  5. dry with materialdried (Na2SO4)
  6. customevaporated in vacuo
  7. customto give an oil
  8. customPurification by flash chromatography (A)
  9. customgave an oil, which
  10. customprecipitated the title compound (0.7 g) m.p. 141°-142.5°

出典と根拠

ORDレコード
ord-c6e5fd534fe44bf9a4f00cf265bd1176
出典データセット
uspto-grants-1988_06
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04749718

反応ノート

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