Nitric Acid → 4-Sulfobenzenediazonium hydroxide

HRID 582948

反応式

HRID 582948 の反応式
[S:1]([OH:11])(=[O:10])([C:3]1[CH:8]=[CH:7][C:6]([NH2:9])=[CH:5][CH:4]=1)=[O:2].[N+:12]([O-])(O)=O.N([O-])=O.[Na+]>O>[OH-:2].[S:1]([C:3]1[CH:4]=[CH:5][C:6]([N+:9]#[N:12])=[CH:7][CH:8]=1)([OH:11])(=[O:10])=[O:2]

参加物

5

実験手順

Two hundred grams of CB-A is added to a solution of 10.1 g sulfanilic acid and 6.23 g of concentrated nitric acid in 21 g of water. A solution of 4.87 g of NaNO2 in 10 g of water is added to the rapidly stirring mixture. 4Sulfobenzenediazonium hydroxide inner salt is formed in situ, which reacts with the carbon black. After 15 minutes, the dispersion is dried in an oven at 125 C.

出典と根拠

ORDレコード
ord-bd5d9244c8a54f16a91ec9a7ce4eb2ef
出典データセット
uspto-grants-1999_07
特許番号
US05928723

関連ノート

読み込み中…