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HRID 583111作成日：2026年10月26日
N-benzyloxycarbonyl-3-[3-(4-formylpiperazin-1-yl)-propoxy]-4-methoxybenzylamine → 3-(3-(4-Formylpiperazin-1-yl)-propoxy]-4-methoxybenzylamine
https://huagongshe.com/reaction/583111
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | N-benzyloxycarbonyl-3-[3-(4-formylpiperazin-1-yl)-propoxy]-4-methoxybenzylamine | HCID 21584186 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 3-(3-(4-Formylpiperazin-1-yl)-propoxy]-4-methoxybenzylamine | HCID 19689424 | 85% |
反応手順
A mixture comprising 30.4 g of N-benzyloxycarbonyl-3-[3-(4-formylpiperazin-1-yl)-propoxy]-4-methoxybenzylamine, 3.1 g of 5% palladium carbon and 300 ml of ethanol, was stirred at 60° C. for 9 hours under a hydrogen atmosphere. Palladium carbon was filtered off, and then the filtrate was distilled off under reduced pressure to obtain 17.99 g of the above-identified compound as slightly brown oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05929074 |
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| 出典データセット | uspto-grants-1999_07 |
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| ORD ID | ord-d982800720d6455987588f91bb211934 |
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| 出典メモ | uspto-grants-1999_07 |
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