Iodoethane → 4-(4-Chloro-3-trifluoromethyl-phenyl)-1-ethyl-piperidine

HRID 584055ノート

反応式

HRID 584055 の反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[C:14]([F:17])([F:16])[F:15].I[CH2:19][CH3:20]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:13][CH2:12][N:11]([CH2:19][CH3:20])[CH2:10][CH2:9]2)=[CH:4][C:3]=1[C:14]([F:17])([F:15])[F:16]

参加物

3

反応物 2

HCID 6340IodoethaneHCID 166793174-[4-Chloro-3-(trifluoromethyl)phenyl]piperidine

生成物 1

HCID 223451894-(4-Chloro-3-trifluoromethyl-phenyl)-1-ethyl-piperidine

実験手順

Beginning with 4-(4-Chloro-3-trifluoromethyl-phenyl)-piperidine and iodoethane, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 291 (M+, 6), 278 (29), 277 (11), 276 (bp), 70 (50).

後処理

  1. customthe title compound was recovered by the procedure

出典と根拠

ORDレコード
ord-f36be6d835f14255a13beaa52b0d19b0
出典データセット
uspto-grants-2005_08
特許番号
US06924374B2

反応ノート

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