Allyl bromide → 1-Allyl-4-(4-Methyl-3-nitro-phenyl)-piperazine

HRID 584060

反応式

HRID 584060 の反応式
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].[CH2:17](Br)[CH:18]=[CH2:19]>>[CH2:19]([N:11]1[CH2:10][CH2:9][N:8]([C:5]2[CH:6]=[CH:7][C:2]([CH3:1])=[C:3]([N+:14]([O-:16])=[O:15])[CH:4]=2)[CH2:13][CH2:12]1)[CH:18]=[CH2:17]

参加物

3

反応物 2

HCID 7841Allyl bromideHCID 47388041-(4-Methyl-3-nitrophenyl)piperazine

生成物 1

HCID 223451921-Allyl-4-(4-Methyl-3-nitro-phenyl)-piperazine

実験手順

Beginning with 1-(4-methyl-3-nitro-phenyl)-piperazine and allylbromide, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 261 (M+, 60), 96 (70), 69 (bp), 68 (48), 56 (73).

後処理

  1. customthe title compound was recovered by the procedure

出典と根拠

ORDレコード
ord-61a497f5e24c4051b5828b53b7df4380
出典データセット
uspto-grants-2005_08
特許番号
US06924374B2

関連ノート

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