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Acetic Acid → methyl 1-formyl-7-(4-propoxyphenyl)-2,3-dihydro-1H-1-benzazepine-4-carboxylate

HRID 586869
ノート
印刷プレビュー

反応式

HRID 586869 の反応式
[C:1](O)(=[O:3])C.C(O)=O.[CH2:8]([O:11][C:12]1[CH:17]=[CH:16][C:15]([C:18]2[CH:19]=[CH:20][C:21]3[NH:27][CH2:26][CH2:25][C:24]([C:28]([O:30][CH3:31])=[O:29])=[CH:23][C:22]=3[CH:32]=2)=[CH:14][CH:13]=1)[CH2:9][CH3:10].C(OC=O)=O>C1COCC1>[CH:1]([N:27]1[C:21]2[CH:20]=[CH:19][C:18]([C:15]3[CH:14]=[CH:13][C:12]([O:11][CH2:8][CH2:9][CH3:10])=[CH:17][CH:16]=3)=[CH:32][C:22]=2[CH:23]=[C:24]([C:28]([O:30][CH3:31])=[O:29])[CH2:25][CH2:26]1)=[O:3]
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

6

反応物 4

HCID 176Acetic AcidHCID 284Formic AcidHCID 9548680Formic anhydrideHCID 22328960methyl 7-(4-propoxyphenyl)-2,3-dihydro-1H-1-benzazepine-4-carboxylate

生成物 1

HCID 22328923methyl 1-formyl-7-(4-propoxyphenyl)-2,3-dihydro-1H-1-benzazepine-4-carboxylate

試薬・触媒・溶媒 1

HCID 8028
Tetrahydrofuran
溶媒
3 回

反応条件

温度
60 °C

実験手順

To anhydrous acetic acid (0.65 ml) was added formic acid (0.32 ml) at 0° C., and the mixture was stirred at 60° C. for 2 hours, air-cooled and diluted with THF (10 ml). In THF (10 ml) was dissolved methyl 7-(4 propoxyphenyl)-2,3-dihydro-1H-1-benzazepine-4-carboxylate (520 mg), and the solution was added dropwise to the previously prepared solution of formic anhydride in THF, at 0° C. The mixture was stirred at room temperature for 1.5 hours. The solvent was evaporated under reduced pressure, and the residue was diluted with ethyl acetate, washed with saturated sodium hydrogen carbonate solution, water and saturated brine, and dried with anhydrous magnesium sulfate. The solvent was evaporated under reduced pressure to give crystals, which were washed with ethyl acetate/hexane to give methyl 1-formyl-7-(4-propoxyphenyl)-2,3-dihydro-1H-1-benzazepine-4-carboxylate (563 mg) as white crystals.

後処理

  1. temperatureair-cooled
  2. stirringThe mixture was stirred at room temperature for 1.5 hours
  3. customThe solvent was evaporated under reduced pressure
  4. additionthe residue was diluted with ethyl acetate
  5. washwashed with saturated sodium hydrogen carbonate solution, water and saturated brine
  6. dry with materialdried with anhydrous magnesium sulfate
  7. customThe solvent was evaporated under reduced pressure
  8. customto give crystals, which
  9. washwere washed with ethyl acetate/hexane

出典と根拠

ORDレコード
ord-e324cb41e2f14621bb6eb031d6442913
出典データセット
uspto-grants-2005_08
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US06936602B1

反応ノート

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