HCID 11667292、化合物 → HCID 14018969、化合物
反応式
C([O:8][C:9]1[CH:25]=[CH:24][C:12]([CH2:13][CH2:14][N:15]([CH3:23])[C:16](=[O:22])[O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[CH:11][CH:10]=1)C1C=CC=CC=1>CO.[Pd]>[OH:8][C:9]1[CH:10]=[CH:11][C:12]([CH2:13][CH2:14][N:15]([CH3:23])[C:16](=[O:22])[O:17][C:18]([CH3:20])([CH3:21])[CH3:19])=[CH:24][CH:25]=1参加物
4
実験手順
To a solution of 1.13 g (3.32 mmol) of tert-butyl 4-(benzyloxy)phenethyl(methyl)carbamate in 15 mL of methanol was added 35 mg of 10% palladium on carbon. The reaction was stirred under a hydrogen balloon atmosphere for 6 h, filtered through celite and evaporated to give tert-butyl 4-hydroxyphenethyl(methyl)carbamate as a colorless oil which was subsequently used without purification.
後処理
- filtrationfiltered through celite
- customevaporated
出典と根拠
- ORDレコード
- ord-fd446867fb964e2ba8c7a5bc92fb991a
- 出典データセット
- uspto-grants-2016_01
- 特許番号
- US09227918B2
反応ノート
読み込み中…