Ammonia → HCID 178463316、化合物

HRID 59011

反応式

HRID 59011 の反応式
Cl.[CH2:2]([N:4]([CH:12]([CH3:14])[CH3:13])[C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[CH:7][CH:6]=1)[CH3:3].[C:15]1([OH:23])[CH:22]=[C:20]([CH3:21])[CH:19]=[C:17]([OH:18])[CH:16]=1.[NH3:24].S(OOS([O-])(=O)=O)([O-])(=O)=O.[NH4+:35].[NH4+].[CH2:37](O)[CH3:38]>O>[CH2:2]([N:4]([CH:12]([CH3:13])[CH3:14])[C:5]1[CH:10]=[CH:9][C:8]([NH:11][C:22]2[C:15](=[O:23])[CH:16]=[C:17]([OH:18])[C:19](=[N:24][C:5]3[CH:10]=[CH:9][C:8]([N:35]([CH2:37][CH3:38])[CH:12]([CH3:14])[CH3:13])=[CH:7][CH:6]=3)[C:20]=2[CH3:21])=[CH:7][CH:6]=1)[CH3:3]

参加物

7

反応物 5

HCID 222AmmoniaHCID 702EthanolHCID 10436OrcinolHCID 62648Ammonium PersulfateHCID 16211123N-Ethyl-N-isopropyl-p-phenylenediamine hydrochloride

生成物 1

HCID 178463316HCID 178463316、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

To a solution of 0.002 mol (429 mg) of N-ethyl-N-isopropyl-4-aminoaniline hydrochloride and 0.001 mol (124 mg) of orcinol in 2 ml of water and 6 ml of ethanol brought to a pH of 9.5 with a solution of 20% aqueous ammonia, 0.002 mol (456 mg) of ammonium persulfate dissolved in 1 ml of water is added dropwise. The temperature is held below 30° C. during the addition. At the end of the addition, the precipitate formed is filtered and washed with water.

後処理

  1. additionis added dropwise
  2. additionThe temperature is held below 30° C. during the addition
  3. additionAt the end of the addition
  4. customthe precipitate formed
  5. filtrationis filtered
  6. washwashed with water

出典と根拠

ORDレコード
ord-4cf052ea8c254f09bf3992e6e71354c9
出典データセット
uspto-grants-2016_09
特許番号
US09439844B2

関連ノート

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