反応式
[NH:1]1[C:11](=[O:12])[C:10]2[NH:9][C:7](=[O:8])[NH:6][C:5]=2[NH:4][C:2]1=[O:3].[OH-].[Na+:14]>>[C:10]12[NH:9][C:7](=[O:8])[N-:6][C:5]=1[NH:4][C:2]([NH:1][C:11]2=[O:12])=[O:3].[Na+:14]参加物
3
反応条件
- 温度
- 70 °C
実験手順
Monosodium urate (MSU) crystals were prepared by dissolving 1.68 g of uric acid in 500 mL of 0.01 M NaOH and heating to 70° C.55,56 NaOH was added as required to maintain the pH between 7.1 and 7.2 and the solution was filtered and incubated at room temperature with slow stirring for 24 hours.
後処理
- temperatureto maintain the pH between 7.1 and 7.2
- filtrationthe solution was filtered
- customincubated at room temperature
出典と根拠
- ORDレコード
- ord-5602e7726f004a31bc1863d79fabac39
- 出典データセット
- uspto-grants-2016_01
- 特許番号
- US09238018B2
関連ノート
読み込み中…