HCID 89768100、化合物 → HCID 89767941、化合物
反応式
C([O:8][C:9]1[CH:21]=[CH:20][C:12]2[C:13]([C:16]([O:18][CH3:19])=[O:17])=[CH:14][O:15][C:11]=2[CH:10]=1)C1C=CC=CC=1>[Pd].CO>[OH:8][C:9]1[CH:21]=[CH:20][C:12]2[CH:13]([C:16]([O:18][CH3:19])=[O:17])[CH2:14][O:15][C:11]=2[CH:10]=1参加物
4
実験手順
To a mixture of methyl 6-(benzyloxy)-1-benzofuran-3-carboxylate (10 g) and MeOH (200 mL) was added 10% Pd—C (2 g). The mixture was stirred under hydrogen atmosphere overnight. The catalyst was removed by filtration. The filtrate was concentrated in vacuo to give the title compound (7.08 g).
後処理
- customThe catalyst was removed by filtration
- concentrationThe filtrate was concentrated in vacuo
出典と根拠
- ORDレコード
- ord-68e75194a4544eb6812f21222fb6f7f2
- 出典データセット
- uspto-grants-2016_01
- 特許番号
- US09238639B2
反応ノート
読み込み中…