Oxalyl chloride → 4-(Bromomethyl)benzoyl isocyanate
反応式
[Br:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([NH2:9])=[O:8])=[CH:5][CH:4]=1.C(Cl)(=O)[C:13](Cl)=[O:14]>C(Cl)CCl>[Br:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([N:9]=[C:13]=[O:14])=[O:8])=[CH:5][CH:4]=1参加物
4
実験手順
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 4-(bromomethyl)benzamide (0.200 g), oxalyl chloride (0.012 mL) and EDC (15 mL) to afford 0.150 g of the desired product.
後処理
- customThe title compound was prepared
出典と根拠
- ORDレコード
- ord-407fd253c6b44db9b13486776b9d965c
- 出典データセット
- uspto-grants-2016_09
- 特許番号
- US09439890B2
反応ノート
読み込み中…