Isoprene → Isoprene acrylonitrile
反応式
[CH2:1]=[CH:2][C:3](=[CH2:5])[CH3:4].Cl[CH:7]([CH3:10])[C:8]#[N:9]>>[CH2:1]=[CH:2][C:3](=[CH2:4])[CH3:5].[C:8](#[N:9])[CH:7]=[CH2:10]参加物
3
反応条件
- 温度
- 80 °C
実験手順
Then, were added thereto 68.2 parts of isoprene and 1.79 parts of 2-chloropropionitrile as an organic halide and stirred under heating at 80° C. to conduct a polymerization reaction. After 137 hours, the same post-treatment as in Example 1 was carried out to give a random (isoprene/acrylonitrile) copolymer. The conversion rate of isoprene was 84% and the conversion rate of acrylonitrile was 79%. The analysis results of the random (isoprene/acrylonitrile) polymer obtained are shown in Table 3. The polymer was confirmed to have a chlorine atom at the terminal of the polymer chain.
後処理
- additionThen, were added
- customa polymerization reaction
出典と根拠
- ORDレコード
- ord-60e0a25855b74722ac70ab07752689e7
- 出典データセット
- uspto-grants-2016_01
- 特許番号
- US09243100B2
反応ノート
読み込み中…