Isoprene → Isoprene acrylonitrile

HRID 595617

反応式

HRID 595617 の反応式
[CH2:1]=[CH:2][C:3](=[CH2:5])[CH3:4].Cl[CH:7]([CH3:10])[C:8]#[N:9]>>[CH2:1]=[CH:2][C:3](=[CH2:4])[CH3:5].[C:8](#[N:9])[CH:7]=[CH2:10]

参加物

3

反応物 2

HCID 6557IsopreneHCID 5192252-Chloropropionitrile

生成物 1

HCID 168239Isoprene acrylonitrile

反応条件

温度
80 °C

実験手順

Then, were added thereto 68.2 parts of isoprene and 1.79 parts of 2-chloropropionitrile as an organic halide and stirred under heating at 80° C. to conduct a polymerization reaction. After 137 hours, the same post-treatment as in Example 1 was carried out to give a random (isoprene/acrylonitrile) copolymer. The conversion rate of isoprene was 84% and the conversion rate of acrylonitrile was 79%. The analysis results of the random (isoprene/acrylonitrile) polymer obtained are shown in Table 3. The polymer was confirmed to have a chlorine atom at the terminal of the polymer chain.

後処理

  1. additionThen, were added
  2. customa polymerization reaction

出典と根拠

ORDレコード
ord-60e0a25855b74722ac70ab07752689e7
出典データセット
uspto-grants-2016_01
特許番号
US09243100B2

関連ノート

読み込み中…