反応式
[CH2:1]=[CH:2][C:3](=[CH2:5])[CH3:4].[C:6](#[N:9])[CH:7]=[CH2:8]>>[CH2:1]=[CH:2][C:3](=[CH2:4])[CH3:5].[C:6](#[N:9])[CH:7]=[CH2:8]参加物
3
実験手順
Then, were added thereto 68.2 parts of isoprene and 1.79 parts of 2-chloropropionitrile as an organic halide, and stirred under heating at 80° C. to conduct a polymerization reaction. After 114 hours, the glass reaction vessel was cooled in a dry ice-methanol bath, and the volatiles were distilled off under reduced pressure to give a random (isoprene/acrylonitrile) copolymer. The conversion rate of isoprene was 84% and the conversion rate of acrylonitrile was 76%. The analysis results of the random (isoprene/acrylonitrile) polymer obtained are shown in Table 5. The polymer was confirmed to have a chlorine atom at the terminal of the polymer chain.
出典と根拠
- ORDレコード
- ord-b420f60afc9f41019e26bed48f0ac137
- 出典データセット
- uspto-grants-2016_01
- 特許番号
- US09243100B2
関連ノート
読み込み中…