Hydrogen Sulfide → Di(1-naphthyl)sulfide
反応式
[SH2:1].Br[C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=1>>[C:3]1([S:1][C:11]2[C:12]3[C:7](=[CH:6][CH:5]=[CH:4][CH:3]=3)[CH:8]=[CH:9][CH:10]=2)[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=1参加物
3
実験手順
By a procedure similar to that described in Example 14, hydrogen sulphide is passed into 20 g (0.1 mole) of molten 1-bromonaphthalene at a temperature of 220°-230° C for seven hours to obtain by distillation in vacuum (1 mm Hg) 7.5 g (52 percent by weight) of di(1-naphthyl)sulphide. The conversion is 82.5 percent by weight.
出典と根拠
- ORDレコード
- ord-643085b566064d88b38c1e26002baa4b
- 出典データセット
- uspto-grants-1977_03
- 特許番号
- US04010210
反応ノート
読み込み中…