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Dimethyldithiocarbamic acid, dimethylamine → alpha-(1-Nitroethyl)benzyl dimethyldithiocarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| 反応物 | (2-Nitro-2-propenyl)benzene | HCID 575754 | — |
| 溶媒 | Carbon Disulfide | HCID 6348 | — |
| 生成物 | alpha-(1-Nitroethyl)benzyl dimethyldithiocarbamate | HCID 21324624 | — |
反応手順
As in Example 17, reaction of (2-nitro-2-propenyl)benzene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide, gave α-(1-nitroethyl)benzyl dimethyldithiocarbamate melting at 92° C.-94° C. when recrystallized without heating from acetone-ethanol solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04011230 |
| 出典データセット | uspto-grants-1977_03 |
| ORD ID | ord-42b83970ab794375977e587eb15f3827 |
| 出典メモ | uspto-grants-1977_03 |