huagongshe.com
HRID596499

反应详情

EQUATION

反应方程式

HRID 596499 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=S)[S-].C[NH2+]C
HCID11728

Dimethyldithiocarbamic acid, dimethylamine

C5H14N2S2

结构：C=C(Cc1ccccc1)[N+](=O)[O-]
HCID575754

(2-Nitro-2-propenyl)benzene

C9H9NO2

PRODUCTS

生成物

1
结构：CC(C(SC(=S)N(C)C)c1ccccc1)[N+](=O)[O-]
HCID21324624

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：S=C=S
溶剂HCID6348

Carbon disulfide

CS2

PROCEDURE

实验过程

As in Example 17, reaction of (2-nitro-2-propenyl)benzene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide, gave α-(1-nitroethyl)benzyl dimethyldithiocarbamate melting at 92° C.-94° C. when recrystallized without heating from acetone-ethanol solution.