Sodium Hydroxide → 1-Amino-2-nitro-4-methoxyethylthiobenzene
反応式
C([NH:4][C:5]1[CH:10]=[CH:9][C:8]([S:11][CH2:12][CH2:13][O:14][CH3:15])=[CH:7][C:6]=1[N+:16]([O-:18])=[O:17])(=O)C.[OH-].[Na+]>CO>[NH2:4][C:5]1[CH:10]=[CH:9][C:8]([S:11][CH2:12][CH2:13][O:14][CH3:15])=[CH:7][C:6]=1[N+:16]([O-:18])=[O:17]参加物
4
実験手順
1.4 G. of 1-acetamido-2-nitro-4-methoxyethylthiobenzene is treated with 3 ml. 5N sodium hydroxide and 6 ml. methanol in the steam bath for about 15 minutes. The mixture is stripped under vacuum and the residue extracted with chloroform. The dried extracts are evaporated giving 1-amino-2-nitro-4-methoxyethylthiobenzene as a red crystalline solid.
後処理
- extractionthe residue extracted with chloroform
- customThe dried extracts are evaporated
出典と根拠
- ORDレコード
- ord-51ceb430a2114c90a8964a7725cdd469
- 出典データセット
- uspto-grants-1977_03
- 特許番号
- US04011320
反応ノート
読み込み中…