1-Iodopropane → 4(1H)-Pyridazinone, 3,5-diphenyl-1-propyl-

反応式

[CH2:1](I)[CH2:2][CH3:3].[C:5]1([C:11]2[C:16](=[O:17])[C:15]([C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)=[CH:14][NH:13][N:12]=2)[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1>>[C:5]1([C:11]2[C:16](=[O:17])[C:15]([C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=3)=[CH:14][N:13]([CH2:1][CH2:2][CH3:3])[N:12]=2)[CH:6]=[CH:7][CH:8]=[CH:9][CH:10]=1

参加物

反応物 2

HCID 336431-Iodopropane

HCID 6192033,5-Diphenyl-1H-pyridazin-4-one

生成物 1

HCID 122629924(1H)-Pyridazinone, 3,5-diphenyl-1-propyl-収率 95%

実験手順

Propyl iodide was reacted with 3,5-diphenyl-4(1H)-pyridazinone according to the process of Example 4 to produce 3,5-diphenyl-1-propyl-4(1H)-pyridazinone, m.p. 94°-96° C. in 95% yield.

出典と根拠

ORDレコード: ord-0cf446f0cba148ff9eac7f15468e9f02
出典データセット: uspto-grants-1977_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04013658

反応ノート

読み込み中…