2-Hydroxybenzonitrile → O-2-cyanophenyl dimethylthiocarbamate
反応式
[OH:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#[N:5].[CH3:10][N:11]([CH3:15])[C:12](Cl)=[S:13].[OH-].[K+]>>[CH3:10][N:11]([CH3:15])[C:12](=[S:13])[O:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#[N:5]参加物
4
実験手順
If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.
出典と根拠
- ORDレコード
- ord-0e3bf4991a3f466d9c41ae0105fc4554
- 出典データセット
- uspto-grants-1993_09
- 特許番号
- US05246961
反応ノート
読み込み中…