反応式
[F:1][C:2]1[CH:7]=[CH:6][C:5]([NH2:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[F:12][C:13]1[CH:14]=[C:15]([CH:19]=[C:20]([C:22]([F:25])([F:24])[F:23])[CH:21]=1)[C:16](Cl)=[O:17].S1C=CC=C1C(Cl)=O>>[F:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:16](=[O:17])[C:15]2[CH:19]=[C:20]([C:22]([F:23])([F:24])[F:25])[CH:21]=[C:13]([F:12])[CH:14]=2)=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10]参加物
4
実験手順
4-Fluoro-3-nitro-phenylamine was reacted with 3-fluoro-5-trifluoromethyl-benzoyl chloride according to the procedure of Example 256a substituting 3-fluoro-5-trifluoromethyl-benzoyl chloride for thiophene-2-carbonyl chloride to provide N-(4-Fluoro-3-nitro-phenyl)-3-fluoro-5-trifluoromethyl-benzamide which was then reacted according to the procedures of Examples 256b and 256c to provide the title product.
出典と根拠
- ORDレコード
- ord-0c1e77ae6af04c2180c37813f7fe03c7
- 出典データセット
- uspto-grants-2011_03
- 特許番号
- US07910595B2
関連ノート
読み込み中…