Potassium Carbonate → HCID 19595683、化合物

HRID 612583

反応式

HRID 612583 の反応式
[OH:1][C:2]1[CH:3]=[C:4]([C:12]([O:14][CH3:15])=[O:13])[C:5](=[CH:10][CH:11]=1)[C:6]([O:8][CH3:9])=[O:7].C(=O)([O-])[O-].[K+].[K+].[CH3:22][O:23][C:24]1[CH:31]=[CH:30][C:27]([CH2:28]Cl)=[CH:26][CH:25]=1>CN(C=O)C>[CH3:22][O:23][C:24]1[CH:31]=[CH:30][C:27]([CH2:28][O:1][C:2]2[CH:3]=[C:4]([C:12]([O:14][CH3:15])=[O:13])[C:5](=[CH:10][CH:11]=2)[C:6]([O:8][CH3:9])=[O:7])=[CH:26][CH:25]=1

参加物

5

反応物 3

HCID 11430Potassium CarbonateHCID 699934-Methyloxybenzyl chlorideHCID 89726Dimethyl 4-hydroxyphthalate

生成物 1

HCID 19595683HCID 19595683、化合物

試薬・触媒・溶媒 1

HCID 6228Dimethylformamide溶媒

実験手順

1 eq. of dimethyl 4-hydroxyphthalate, 1.1 eq. of potassium carbonate and 1.1 eq. of 4-methoxybenzyl chloride were stirred in DMF at RT. After 4 days, the mixture was worked up according to a standard procedure. Dimethyl 4-(4-methoxybenzyloxy)phthalate was isolated as a colorless oil. MS: 331 ((M+1)+)

出典と根拠

ORDレコード
ord-6aa64a686a13461fbdec1ab546ad0f32
出典データセット
uspto-grants-1999_12
特許番号
US06005010

関連ノート

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