反応式
[CH3:1][CH:2]([CH:7]([CH3:9])[CH3:8])[C:3](=[CH2:6])[CH:4]=[O:5].[CH2:10]=[CH:11][C:12](=[CH2:14])[CH3:13]>>[CH3:1][CH:2]([C:3]1([CH:4]=[O:5])[CH2:10][CH2:11][C:12]([CH3:14])=[CH:13][CH2:6]1)[CH:7]([CH3:9])[CH3:8]参加物
3
反応条件
- 温度
- 160 °C
実験手順
3,4-Dimethyl-2-methylene-pentanal (550 g, obtained as detailed above) and 393 g of isoprene were charged to a Parr Bomb, heated to 160° C., and aged for 12 hours. The rushed over material provided ˜32% recovery of 1-(1,2-dimethyl-propyl)-4-methyl-cyclohex-3-enecarbaldehyde (415 g).
出典と根拠
- ORDレコード
- ord-3203e99590bb4da6b11acc7689d1cedd
- 出典データセット
- uspto-grants-2016_09
- 特許番号
- US09441185B2
関連ノート
読み込み中…