化工社化工社 化学情報印刷レポート · 研究参考用
Hesperidin → Hesperidin silver
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hesperidin | HCID 10621 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Silver | HCID 23954 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Benzenesulfonic acid, 4-methyl-, silver(1+) salt (1:1) | HCID 85606 | — |
| 生成物 | Hesperidin silver | HCID 131737181 | — |
反応手順
Hesperidin/silver colloidal nanoparticle catalyst is prepared by dissolving 1.65 g hesperidin in a beaker containing 800 ml DI water at room temperature. 1 N NaOH solution with stirring is added to adjust the solution pH to 11. In a separate beaker, 2.2 g silver p-toluenesulfonate is dissolved in 60 ml DI water. The silver ion solution is added to the hesperidin solution with strong stirring. The molar ratio of silver to hesperidin is 1:0.34. The beaker containing the aqueous catalyst solution is placed in a 50° C. water bath for 12 hours to test its stability. After 12 hours the solution is observed and no precipitate is expected indicating that the catalyst is still stable.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09441300B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-d52d89091fb1495d99f897f5da5dbdc4 |
| 出典メモ | uspto-grants-2016_09 |