化工社化工社 化学情報印刷レポート · 研究参考用
Acetyl chloride → Methyl 3-(4-methylphenyl)-2-propenoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | 3-(p-Tolyl)acrylic acid | HCID 15835 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Methyl 3-(4-methylphenyl)-2-propenoate | HCID 589472 | — |
反応手順
A solution of 6.0 g (37.0 mmol) of 4-methylcinnamic acid in 120 ml of anhydrous MeOH was treated with 6 ml of acetyl chloride and stirred at reflux for 18 hours. Evaporation of the MeOH gave the title ester as a white solid, mp 53.5°-57.5° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04499299 |
| 出典データセット | uspto-grants-1985_02 |
| ORD ID | ord-48020e780ce84bf2a68e8cb41673e567 |
| 出典メモ | uspto-grants-1985_02 |