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Ethyl chloroformate → N,N'-bis-(ethoxycarbonyl)-N,N'-bis-(2,2,6,6-tetramethyl-piperidin-4-yl)-hexamethylenediamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl chloroformate | HCID 10928 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 1,6-Bis(2,2,6,6-tetramethyl-4-piperidylamino)hexane | HCID 93419 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N,N'-bis-(ethoxycarbonyl)-N,N'-bis-(2,2,6,6-tetramethyl-piperidin-4-yl)-hexamethylenediamine | HCID 18998995 | — |
反応手順
The N,N'-bis-(ethoxycarbonyl)-N,N'-bis-(2,2,6,6-tetramethyl-piperidin-4-yl)-hexamethylenediamine was prepared by reacting N,N'-bis-(2,2,6,6-tetramethyl-piperidin-4-yl)-hexamethylenediamine with ethyl chlorocarbonate in toluene in the presence of aqueous NaOH and was crystallised from octane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04501837 |
| 出典データセット | uspto-grants-1985_02 |
| ORD ID | ord-75a852042da1470b858a622f8fc14518 |
| 出典メモ | uspto-grants-1985_02 |