Iodoethane → HCID 20370474、化合物

反応式

[CH3:1][N:2]([CH3:19])[C:3](=[O:18])[CH:4]([CH3:17])[N:5]1[CH:9]=[C:8]([CH3:10])[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1.[CH2:20](Br)[CH2:21][CH3:22].[CH2:24](I)C>>[CH2:17]([C:4]([CH2:20][CH2:21][CH3:22])([N:5]1[CH:9]=[C:8]([CH3:10])[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1)[C:3]([N:2]([CH3:1])[CH3:19])=[O:18])[CH3:24]

参加物

反応物 3

HCID 6340Iodoethane

HCID 78401-Bromopropane

HCID 20370501N,N-dimethyl-2-(4-methyl-3-phenyl-1H-pyrazol-1-yl)propanamide

生成物 1

HCID 20370474HCID 20370474、化合物

実験手順

Following the procedure of Example 95, but substituting α-ethyl-N,N,4-trimethyl-3-phenylpyrazole-1-acetamide for N,N,α,4-tetramethyl-3-phenylpyrazole-1-acetamide and propyl bromide for ethyl iodide, there was obtained α-ethyl-N,N,4-trimethyl-3-phenyl-α-propylpyrazole-1-acetamide having a melting point of 147°-148° C.

出典と根拠

ORDレコード: ord-d441b90ad2a847589c4b14ae3862b913
出典データセット: uspto-grants-1978_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04072498

反応ノート

読み込み中…

参加物