Sulfuric Acid → 2,6-Dimethylhydroquinone

HRID 616071

反応式

HRID 616071 の反応式
S(=O)(=O)(O)[OH:2].[CH3:6][C:7]1[CH:13]=[C:12]([CH3:14])[CH:11]=[C:9]([OH:10])[C:8]=1O>>[CH3:6][C:7]1[CH:8]=[C:9]([OH:10])[CH:11]=[C:12]([CH3:14])[C:13]=1[OH:2]

参加物

3

実験手順

By following in the same manner as in Example 56 except that 0.11 g. of strong acidic sulfontype ion exchange resin Amberlyst 15 (manufactured by Rohm and Hass Co.) was used instead of sulfuric acid, 2.55 g. (18.5 m.moles) of 3,5-dimethylcatechol and 1.26 g. (9.1 m.moles) of 2,6-dimethylhydroquinone were obtained. The yield of dihydric alkylphenols was 65.6%.

出典と根拠

ORDレコード
ord-6552ffe34cc045bab2d0743ec152c946
出典データセット
uspto-grants-1978_02
特許番号
US04072722

関連ノート

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