反応式
[C:1]1([CH3:9])[CH:6]=[CH:5][CH:4]=[C:3]([C:7]#[N:8])[CH:2]=1.[ClH:10].[CH2:11]([OH:13])[CH3:12]>>[ClH:10].[CH3:9][C:1]1[CH:2]=[C:3]([CH:4]=[CH:5][CH:6]=1)[C:7](=[NH:8])[O:13][CH2:11][CH3:12]参加物
4
実験手順
Ethyl 3-methylbenzimidate hydrochloride was synthesized in the same manner as in Reference Example 2. That is, m-tolunitrile (25.2 g, 0.215 mol) was treated with hydrogen chloride in ethanol (250 mL) to give 41.7 g (97%) of the target compound as colorless crystals.
出典と根拠
- ORDレコード
- ord-472e9956c224470ca9bd5bd552bcd52d
- 出典データセット
- uspto-grants-1999_09
- 特許番号
- US05948785
関連ノート
読み込み中…