Methane → HCID 21243167、化合物

HRID 621424

反応式

HRID 621424 の反応式
[NH2:1][C:2]1[N:7]=[C:6](N)[N:5]=[C:4]([NH:9][CH:10]2[CH2:12][CH2:11]2)[N:3]=1.C(N([CH2:18][CH3:19])CC)C.[CH4:20].[O:21]1[CH2:25][CH2:24][CH2:23][CH2:22]1>>[CH:10]1([NH:9][C:4]2[N:3]=[C:2]([NH:1][C:22](=[O:21])[CH2:23][CH2:24][CH2:25][CH2:20][CH2:18][CH3:19])[N:7]=[CH:6][N:5]=2)[CH2:12][CH2:11]1

参加物

5

反応物 4

HCID 297MethaneHCID 8028Tetrahydrofuran2 回HCID 8471TriethylamineHCID 47866Cyromazine

生成物 1

HCID 21243167HCID 21243167、化合物

実験手順

To a suspension of 33.2 g of 2,4-diamino-6-cyclopropylamino-1,3,5-triazine and 30.3 g of triethylamine in 800 ml of tetrahydrofuran are slowly added dropwise, at 60° C., 50.9 g of oenanthic acid anhydride dissolved in 100 ml of tetrahydrofuran. The reaction mixture is subsequently stirred overnight at 60° C.; active charcoal is then added and the mixture is filtered hot. The filtrate is concentrated by evaporation, and isopropanol is added. The product is obtained, after filtration and drying, in the form of a white crystalline powder having a melting point of 195°-197° C.

後処理

  1. additionare slowly added dropwise, at 60° C.
  2. filtrationthe mixture is filtered hot
  3. concentrationThe filtrate is concentrated by evaporation, and isopropanol
  4. additionis added
  5. customThe product is obtained
  6. filtrationafter filtration
  7. customdrying, in the form of a white crystalline powder

出典と根拠

ORDレコード
ord-ef5e7859ad19486db3974ffa43406063
出典データセット
uspto-grants-1989_04
特許番号
US04824845

関連ノート

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