反応式
[CH3:1][N:2]([CH3:7])[S:3]([CH3:6])(=[O:5])=[O:4].C([Li])CCC.[F:13][C:14]1[CH:23]=[CH:22][C:17]([C:18](OC)=[O:19])=[C:16]([NH:24][CH3:25])[CH:15]=1>>[F:13][C:14]1[CH:23]=[CH:22][C:17]([C:18](=[O:19])[CH2:6][S:3](=[O:5])(=[O:4])[N:2]([CH3:7])[CH3:1])=[C:16]([NH:24][CH3:25])[CH:15]=1参加物
4
実験手順
In a similar manner to that described in Example 12(a), N,N-dimethylmethanesulphonamide was reacted with n-butyl lithium and the product reacted with methyl 4-fluoro-2-methylaminobenzoate to give the novel compound 1-(4-fluoro-2-methylaminophenyl)-2-(N,N-dimethylsulphamoyl)ethanone, m.p. 120°-124°.
出典と根拠
- ORDレコード
- ord-c24a0e6d7e42499c8d2fc5ebb355d326
- 出典データセット
- uspto-grants-1988_09
- 特許番号
- US04772614
関連ノート
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