Dimethylamine, hydrochloride → HCID 3554384、化合物

HRID 622807ノート

反応式

HRID 622807 の反応式
Cl.[CH3:2][NH:3][CH3:4].[CH3:5][O:6][C:7](=[O:17])[C:8]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=[CH:9]O.[Na]>O>[CH3:5][O:6][C:7](=[O:17])[C:8]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=[CH:9][N:3]([CH3:4])[CH3:2]

参加物

4

反応物 2

HCID 10473Dimethylamine, hydrochlorideHCID 70407058HCID 70407058、化合物

生成物 1

HCID 3554384HCID 3554384、化合物収率 72.2%

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

97 weight-parts of dimethylamine hydrochloride are dissolved in 250 weight-parts of water, and 200 weight-parts of sodium 3-hydroxy-2-phenyl acrylic acid methyl ester are added. The mixture is stirred for 2 hours, and the organic phase is separated and distilled. 148 weight-parts of 3-dimethylamino-2-phenyl acrylic acid methyl ester are obtained, corresponding to a yield of 72.2% of the theory.

後処理

  1. additionare added
  2. customthe organic phase is separated
  3. distillationdistilled

出典と根拠

ORDレコード
ord-42f29bb6a9ac4b9d87ac01e86138f738
出典データセット
uspto-grants-1988_09
特許番号
US04772711

反応ノート

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