Acrylonitrile → 3-Cyclohexene-1-carbonitrile, 3,4-dimethyl-
反応式
[C:1](#[N:4])[CH:2]=[CH2:3].[CH3:5][C:6]([C:8]([CH3:10])=[CH2:9])=[CH2:7]>C1(C)C=CC=CC=1>[CH3:7][C:6]1[CH2:5][CH:2]([C:1]#[N:4])[CH2:3][CH2:9][C:8]=1[CH3:10]参加物
4
実験手順
A solution of acrylonitrile (1 eq.) and 2,3-dimethylbuta-1,3-diene (1.1 eq.) in toluene (2M) was pumped through a heated coil reactor at 240° C. with a residence time of 10 minutes. The resulting mixture was concentrated under reduced pressure and yielded the product as colorless oil (87% yield).
後処理
- concentrationThe resulting mixture was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-b54ff47562704e93b1e2067e66822843
- 出典データセット
- uspto-grants-2016_04
- 特許番号
- US09303232B2
反応ノート
読み込み中…