反応式
[Cl:1][C:2]1[C:7]([O:8][CH2:9][CH3:10])=[CH:6][C:5]([I:11])=[CH:4][C:3]=1[OH:12].Br[CH:14]([CH2:17][CH3:18])[CH2:15][CH3:16]>>[Cl:1][C:2]1[C:3]([O:12][CH:14]([CH2:17][CH3:18])[CH2:15][CH3:16])=[CH:4][C:5]([I:11])=[CH:6][C:7]=1[O:8][CH2:9][CH3:10]参加物
3
実験手順
2-Chloro-1-ethoxy-5-iodo-3-(pentan-3-yloxy)benzene (8) (1.2 g, 79%) was prepared from 2-chloro-3-ethoxy-5-iodophenol (7) (1.1 g, 3.7 mmol) using a procedure essentially the same as in step (i) for AAA-001 except that 3-bromopentane was used instead of cyclopentyl bromide.
出典と根拠
- ORDレコード
- ord-8181d3479b6a417fa4adc534e9103e2d
- 出典データセット
- uspto-grants-2016_09
- 特許番号
- US09447028B2
関連ノート
読み込み中…