HCID 86674754、化合物 → 2-Amino-2-ethyl-N-methyl-butyramide

HRID 632079

反応式

HRID 632079 の反応式
[CH3:1][NH:2][C:3]([C:5]([NH:10]C(=O)OC(C)(C)C)([CH2:8][CH3:9])[CH2:6][CH3:7])=[O:4]>Cl.C(OCC)(=O)C>[NH2:10][C:5]([CH2:8][CH3:9])([CH2:6][CH3:7])[C:3]([NH:2][CH3:1])=[O:4]

参加物

4

反応物 1

HCID 86674754HCID 86674754、化合物

生成物 1

HCID 798103702-Amino-2-ethyl-N-methyl-butyramide収率 75%

試薬・触媒・溶媒 2

HCID 313Hydrochloric Acid溶媒HCID 8857Ethyl Acetate溶媒

実験手順

A mixture of tert-butyl 3-(methylcarbamoyl)pentan-3-ylcarbamate (0.18 g, 0.74 mmol) in 10 ml saturated hydrochloride in ethyl acetate was stirred for 60 min at room temperature. Then the solution was evaporated to dryness to obtain the product (80 mg, 75%) as a light yellow solid; MS (LC/MS): 145.2 [M+H]+.

後処理

  1. customThen the solution was evaporated to dryness

出典と根拠

ORDレコード
ord-c87266b78f9b4f709056706310a5c905
出典データセット
uspto-grants-2016_04
特許番号
US09321727B2

関連ノート

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