化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → HCID 15382693、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| 反応物 | N-benzoyl-2'-deoxyadenosine | HCID 107558 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | HCID 15382693 | HCID 15382693 | — |
反応手順
The synthesis of this product is carried out by reacting 1 eq of p-nitrobenzoyl chloride with 6-N-benzoyldeoxyadenosine for 4 hours in pyridine. After hydrolysis of the excess reagent, partial evaporation of the pyridine, extraction and evaporation of the chloroformic phase, the product is obtained by column chromatography (elution 4% methanol).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06187914B1 |
| 出典データセット | uspto-grants-2001_02 |
| ORD ID | ord-5abaca9d871242a3abe42dc791ab9001 |
| 出典メモ | uspto-grants-2001_02 |