Hydrochloric Acid → Methyl 3-{[2-(diaminomethyleneamino)thiazol-4-YL]methylthio}propanimidate

反応式

[C:1]([CH2:3][CH2:4][S:5][CH2:6][C:7]1[N:8]=[C:9]([N:12]=[C:13]([NH2:15])[NH2:14])[S:10][CH:11]=1)#[N:2].Cl.[CH2:17]=[O:18]>>[NH2:15][C:13](=[N:12][C:9]1[S:10][CH:11]=[C:7]([CH2:6][S:5][CH2:4][CH2:3][C:1](=[NH:2])[O:18][CH3:17])[N:8]=1)[NH2:14]

参加物

反応物 3

HCID 313Hydrochloric Acid

HCID 712Formaldehyde

HCID 50752593-(2-(Diaminomethyleneamino)thiazol-4-yl)methylthio)propiononitrile

生成物 1

HCID 12881442Methyl 3-{[2-(diaminomethyleneamino)thiazol-4-YL]methylthio}propanimidate

実験手順

reacting the compound produced in step (b) with hydrogen chloride and methanal to obtain the compound methyl 3-[[[2-[(diaminomethylene)amino]-4-thiazolyl]-methyl]thio]propionimidate isolating and drying said compound; and

出典と根拠

ORDレコード: ord-5a1e6b2a0e6647e7930c01bfbef2b1d7
出典データセット: uspto-grants-1986_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04609737

反応ノート

読み込み中…